Difference between revisions of "SOI grating definition"

From OptoelectronicsWiki
Jump to: navigation, search
(Dose/Duty Cycle Analysis with Proximity Effect Observations)
Line 23: Line 23:
 
         N2 Dry    DO NOT RINSE WITH DI
 
         N2 Dry    DO NOT RINSE WITH DI
 
     Grating Etch       
 
     Grating Etch       
         AFM Calibration Recommended    
+
         AFM etch depth calibration recommended    
         Single Step Bosch Etch Process - JTB_GR   "Etch rate varies with temperature
+
         Single Step Bosch Etch Process - JTB_GR
 
         Rates:
 
         Rates:
 
         ~170nm/min w/o Sanovac 5
 
         ~170nm/min w/o Sanovac 5
Line 37: Line 37:
 
==Future Untested Processes==
 
==Future Untested Processes==
 
===Sweeper Two Etch Depth Grating Process (INCOMPLETE)===
 
===Sweeper Two Etch Depth Grating Process (INCOMPLETE)===
Standad EBL Spin,Bake, Exposure, Develop
+
    Standard Process
 
+
        Pre-clean: Remove native oxide and/or dielectric hardmask
     Spin AZ4210 (4000rpm, 30sec)
+
            HF dip
    Pre-Exposure Bake (95C, 1min)
+
        Ebeam PR spin coat (2:1 ZEP)
 
+
            ACE,ISO,DI 
Lithography  
+
            PEII - O2 Descum (100W, 300mTorr, 60sec) 
30    GCA Stepper / Autostepper
+
            Dehydration Bake (150C, 5min) 
    Exposure: 3sec / 1sec (NEEDS CALIBRATION)
+
            N2 Gun (1min)    Cools and cleans wafer
    Focus Offset: 0 (NEEDS CALIBRATION)
+
            Spin 2:1 ZEP (3000rpm, 30sec) - Recipe 5    ~225nm, Use a filtered syringe
    NO POST-EXPOSURE BAKE
+
            Pre-Exposure Bake (180C, 4min)    Cover hotplate top to prevent additional particulate
    Develop (AZ400K 1:4 diluted, 1min)
+
        Thermal Au Evaporation     
    DI Rinse
+
            Evaporate 11nm Au
 
+
        Ebeam Writing Conditions     
Partial deep grating etch
+
            4th Lens 
 
+
            Dose 350uC/cm2 (Please be aware this is pitch dependent, but has shown good results over a range of pitches if the substrate is not highly doped)
4210 strip in ISO
+
        Development     
 
+
            Remove Au in wet Au etchant    10s
Shallow grating etch/Complete deep grating etch.
+
            DI Rinse 
 
+
            N2 Dry 
ZEP Strip (1165)
+
            1:1 MIBK:ISO Development - 60s    Use a fresh batch
 +
            9:1 MIBK:ISO Rinse - 15s    DO NOT RINSE WITH DI
 +
            N2 Dry    DO NOT RINSE WITH DI
 +
     Add PR protection layer
 +
        Spin AZ4210 (4000rpm, 30sec)
 +
        Pre-Exposure Bake (95C, 1min)
 +
        Lithography - Pattern a window in the deep etch region
 +
            Litho Tool: GCA Stepper / Autostepper
 +
            Exposure: 3sec / 1sec (NEEDS CALIBRATION)
 +
            Focus Offset: 0 (NEEDS CALIBRATION)
 +
            NO POST-EXPOSURE BAKE
 +
            Develop (AZ400K 1:4 diluted, 1min)
 +
            DI Rinse
 +
    Grating Partial Etch - Etch the difference in depths (deep target - shallow target)     
 +
            AFM etch depth calibration recommended 
 +
            Single step Bosch etch process - JTB_GR
 +
            Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
 +
    Strip PR protection layer       
 +
        Strip AZ4210 in ISO - Should not attack ZEP(2:1)
 +
    Grating Shallow/Finish Deep Etch - Etch the difference in depths (deep target - shallow target)     
 +
            AFM etch depth calibration recommended 
 +
            Single step Bosch etch process - JTB_GR
 +
            Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5

Revision as of 19:20, 27 October 2011

Current Processes

Sweeper Vertical Grating Coupler Process

   Pre-clean: Remove native oxide and/or dielectric hardmask
       HF dip
   Ebeam PR spin coat (2:1 ZEP)
       ACE,ISO,DI   
       PEII - O2 Descum (100W, 300mTorr, 60sec)   
       Dehydration Bake (150C, 5min)   
       N2 Gun (1min)    Cools and cleans wafer
       Spin 2:1 ZEP (3000rpm, 30sec) - Recipe 5    ~225nm, Use a filtered syringe
       Pre-Exposure Bake (180C, 4min)    Cover hotplate top to prevent additional particulate
   Thermal Au Evaporation       
       Evaporate 11nm Au
   Ebeam Writing Conditions       
       4th Lens   
       Dose 350uC/cm2 (Please be aware this is pitch dependent, but has shown good results over a range of pitches if the substrate is not highly doped)
   Development       
       Remove Au in wet Au etchant    10s
       DI Rinse   
       N2 Dry   
       1:1 MIBK:ISO Development - 60s    Use a fresh batch
       9:1 MIBK:ISO Rinse - 15s    DO NOT RINSE WITH DI
       N2 Dry    DO NOT RINSE WITH DI
   Grating Etch       
       AFM etch depth calibration recommended   
       Single Step Bosch Etch Process - JTB_GR
       Rates:
       ~170nm/min w/o Sanovac 5
       ~141nm/min w/ Sanovac 5

Process Development Summary

Dose/Duty Cycle Analysis with Proximity Effect Observations

File:2010-03-01 Grating Update.pptx

File:2010-12-07 Grating Update.pptx

Future Untested Processes

Sweeper Two Etch Depth Grating Process (INCOMPLETE)

   Standard Process
       Pre-clean: Remove native oxide and/or dielectric hardmask
           HF dip
       Ebeam PR spin coat (2:1 ZEP)
           ACE,ISO,DI   
           PEII - O2 Descum (100W, 300mTorr, 60sec)   
           Dehydration Bake (150C, 5min)   
           N2 Gun (1min)    Cools and cleans wafer
           Spin 2:1 ZEP (3000rpm, 30sec) - Recipe 5    ~225nm, Use a filtered syringe
           Pre-Exposure Bake (180C, 4min)    Cover hotplate top to prevent additional particulate
       Thermal Au Evaporation       
           Evaporate 11nm Au
       Ebeam Writing Conditions       
           4th Lens   
           Dose 350uC/cm2 (Please be aware this is pitch dependent, but has shown good results over a range of pitches if the substrate is not highly doped)
       Development       
           Remove Au in wet Au etchant    10s
           DI Rinse   
           N2 Dry   
           1:1 MIBK:ISO Development - 60s    Use a fresh batch
           9:1 MIBK:ISO Rinse - 15s    DO NOT RINSE WITH DI
           N2 Dry    DO NOT RINSE WITH DI
   Add PR protection layer
       Spin AZ4210 (4000rpm, 30sec)
       Pre-Exposure Bake (95C, 1min)
       Lithography - Pattern a window in the deep etch region 
           Litho Tool: GCA Stepper / Autostepper
           Exposure: 3sec / 1sec (NEEDS CALIBRATION)
           Focus Offset: 0 (NEEDS CALIBRATION)
           NO POST-EXPOSURE BAKE
           Develop (AZ400K 1:4 diluted, 1min)
           DI Rinse
   Grating Partial Etch - Etch the difference in depths (deep target - shallow target)      
           AFM etch depth calibration recommended   
           Single step Bosch etch process - JTB_GR
           Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
   Strip PR protection layer        
       Strip AZ4210 in ISO - Should not attack ZEP(2:1)
   Grating Shallow/Finish Deep Etch - Etch the difference in depths (deep target - shallow target)      
           AFM etch depth calibration recommended   
           Single step Bosch etch process - JTB_GR
           Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5