Difference between revisions of "SOI grating definition"

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(Sweeper Two Etch Depth Grating Process (UNTESTED))
(Sweeper Two Etch Depth Grating Process (UNTESTED))
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==Future Untested Processes==
 
==Future Untested Processes==
 
===Sweeper Two Etch Depth Grating Process (UNTESTED)===
 
===Sweeper Two Etch Depth Grating Process (UNTESTED)===
     Standard Process (with conductive polymer)
+
     Oxide Hardmask Deposition - Advanced Vacuum PECVD
         Pre-clean: Remove native oxide and/or dielectric hardmask
+
         40nm Oxide
            HF dip
+
    Ebeam PR spin coat (2:1 ZEP)
        Ebeam PR spin coat (2:1 ZEP)
+
        ACE,ISO,DI   
            ACE,ISO,DI   
+
        PEII - O2 Descum (100W, 300mTorr, 60sec)   
            PEII - O2 Descum (100W, 300mTorr, 60sec)   
+
        Dehydration Bake (150C, 5min)   
            Dehydration Bake (150C, 5min)   
+
        N2 Gun (1min)    Cools and cleans wafer
            N2 Gun (1min)    Cools and cleans wafer
+
        Spin 2:1 ZEP (3000rpm, 30sec) - Recipe 5    ~225nm, Use a filtered syringe
            Spin 2:1 ZEP (3000rpm, 30sec) - Recipe 5    ~225nm, Use a filtered syringe
+
        Pre-Exposure Bake (180C, 4min)    Cover hotplate top to prevent additional particulate
            Pre-Exposure Bake (180C, 4min)    Cover hotplate top to prevent additional particulate
+
    Conductive polymer spin coat
        Conductive polymer spin coat
+
        Aquasave (3000 rpm, 30sec) - Recipe 5
            Aquasave (3000 rpm, 30sec) - Recipe 5
+
        Pre-Exposure bake (90C, 30sec)
            Pre-Exposure bake (90C, 30sec)
+
    Ebeam Writing Conditions       
        Ebeam Writing Conditions       
+
        4th Lens   
            4th Lens   
+
        Dose 350uC/cm2 (Please be aware this is pitch dependent, but has shown good results over a range of pitches if the substrate is not highly doped)
            Dose 350uC/cm2 (Please be aware this is pitch dependent, but has shown good results over a range of pitches if the substrate is not highly doped)
+
    Development       
        Development       
+
        DI Rinse - 60s Removes Aquasave   
            DI Rinse - 60s Removes Aquasave   
+
        N2 Dry   
            N2 Dry   
+
        1:1 MIBK:ISO Development - 60s    Use a fresh batch
            1:1 MIBK:ISO Development - 60s    Use a fresh batch
+
        9:1 MIBK:ISO Rinse - 15s    DO NOT RINSE WITH DI
            9:1 MIBK:ISO Rinse - 15s    DO NOT RINSE WITH DI
+
        N2 Dry    DO NOT RINSE WITH DI
            N2 Dry    DO NOT RINSE WITH DI
+
    AFM Pattern Acknowledgement 
 +
    Hardmask Etch - ICP#2
 +
        Oxide Nano Etch - 110nm/min
 +
    Grating Shallow Etch - Si Deep RIE Etcher (50nm)       
 +
        Single step Bosch etch process - JTB_01
 +
        Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
 
     Add PR protection layer
 
     Add PR protection layer
 
         Spin AZ4210 (4000rpm, 30sec)
 
         Spin AZ4210 (4000rpm, 30sec)
Line 75: Line 80:
 
             Develop (AZ400K 1:4 diluted, 1min)
 
             Develop (AZ400K 1:4 diluted, 1min)
 
             DI Rinse
 
             DI Rinse
     Grating Partial Etch - Etch the difference in depths (deep target - shallow target)       
+
    OPEN OPTION...SHOULD WE RUN A O2 PLASMA CLEAN
 +
     Grating Finish Deep Etch - Etch the difference in depths (deep target - shallow target)       
 
             AFM etch depth calibration recommended   
 
             AFM etch depth calibration recommended   
 
             Single step Bosch etch process - JTB_GR
 
             Single step Bosch etch process - JTB_GR
 
             Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
 
             Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
     Strip PR protection layer       
+
     Strip PR & ZEP (2:1)
        Strip AZ4210 in ISO - Should not attack ZEP(2:1)
+
    Grating Shallow/Finish Deep Etch - Etch the difference in depths (deep target - shallow target)     
+
            AFM etch depth calibration recommended 
+
            Single step Bosch etch process - JTB_GR
+
            Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
+
    Strip ZEP (2:1)
+
 
         1165 Soak at 80C - 10min
 
         1165 Soak at 80C - 10min
 
         PEII - O2 Descum (100W, 300mTorr, 60sec)
 
         PEII - O2 Descum (100W, 300mTorr, 60sec)

Revision as of 15:04, 19 December 2011

Back to Process_Hybrid_Silicon.

Past Processes

Sweeper Vertical Grating Coupler Process

   Pre-clean: Remove native oxide and/or dielectric hardmask
       HF dip
   Ebeam PR spin coat (2:1 ZEP)
       ACE,ISO,DI   
       PEII - O2 Descum (100W, 300mTorr, 60sec)   
       Dehydration Bake (150C, 5min)   
       N2 Gun (1min)    Cools and cleans wafer
       Spin 2:1 ZEP (3000rpm, 30sec) - Recipe 5    ~225nm, Use a filtered syringe
       Pre-Exposure Bake (180C, 4min)    Cover hotplate top to prevent additional particulate
   Thermal Au Evaporation       
       Evaporate 11nm Au
   Ebeam Writing Conditions       
       4th Lens   
       Dose 350uC/cm2 (Please be aware this is pitch dependent, but has shown good results over a range of pitches if the substrate is not highly doped)
   Development       
       Remove Au in wet Au etchant    10s
       DI Rinse   
       N2 Dry   
       1:1 MIBK:ISO Development - 60s    Use a fresh batch
       9:1 MIBK:ISO Rinse - 15s    DO NOT RINSE WITH DI
       N2 Dry    DO NOT RINSE WITH DI
   Grating Etch       
       AFM etch depth calibration recommended   
       Single Step Bosch Etch Process - JTB_GR
       Rates:
       ~170nm/min w/o Sanovac 5
       ~141nm/min w/ Sanovac 5
   Strip ZEP (2:1)
       1165 Soak at 80C - 10min
       PEII - O2 Descum (100W, 300mTorr, 60sec)

Standard Hybrid Si Process

link to .xls

Process Development Summary

Dose/Duty Cycle Analysis with Proximity Effect Observations

File:2010-03-01 Grating Update.pptx

File:2010-12-07 Grating Update.pptx

Future Untested Processes

Sweeper Two Etch Depth Grating Process (UNTESTED)

   Oxide Hardmask Deposition - Advanced Vacuum PECVD 
       40nm Oxide
   Ebeam PR spin coat (2:1 ZEP)
       ACE,ISO,DI   
       PEII - O2 Descum (100W, 300mTorr, 60sec)   
       Dehydration Bake (150C, 5min)   
       N2 Gun (1min)    Cools and cleans wafer
       Spin 2:1 ZEP (3000rpm, 30sec) - Recipe 5    ~225nm, Use a filtered syringe
       Pre-Exposure Bake (180C, 4min)    Cover hotplate top to prevent additional particulate
   Conductive polymer spin coat
       Aquasave (3000 rpm, 30sec) - Recipe 5
       Pre-Exposure bake (90C, 30sec)
   Ebeam Writing Conditions       
       4th Lens   
       Dose 350uC/cm2 (Please be aware this is pitch dependent, but has shown good results over a range of pitches if the substrate is not highly doped)
   Development       
       DI Rinse - 60s Removes Aquasave   
       N2 Dry   
       1:1 MIBK:ISO Development - 60s    Use a fresh batch
       9:1 MIBK:ISO Rinse - 15s    DO NOT RINSE WITH DI
       N2 Dry    DO NOT RINSE WITH DI
   AFM Pattern Acknowledgement   
   Hardmask Etch - ICP#2
       Oxide Nano Etch - 110nm/min
   Grating Shallow Etch - Si Deep RIE Etcher (50nm)        
       Single step Bosch etch process - JTB_01
       Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
   Add PR protection layer
       Spin AZ4210 (4000rpm, 30sec)
       Pre-Exposure Bake (95C, 1min)
       Lithography - Pattern a window in the deep etch region 
           Litho Tool: GCA Stepper / Autostepper
           Exposure: 3sec / 1sec (NEEDS CALIBRATION)
           Focus Offset: 0 (NEEDS CALIBRATION)
           NO POST-EXPOSURE BAKE
           Develop (AZ400K 1:4 diluted, 1min)
           DI Rinse
   OPEN OPTION...SHOULD WE RUN A O2 PLASMA CLEAN
   Grating Finish Deep Etch - Etch the difference in depths (deep target - shallow target)      
           AFM etch depth calibration recommended   
           Single step Bosch etch process - JTB_GR
           Rates: ~170nm/min w/o Sanovac 5, ~141nm/min w/ Sanovac 5
   Strip PR & ZEP (2:1)
       1165 Soak at 80C - 10min
       PEII - O2 Descum (100W, 300mTorr, 60sec)