Difference between revisions of "Measurements"

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(Atomic Force Microscopy (AFM))
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= Materials Characterization =
 
= Materials Characterization =
 
== Atomic Force Microscopy (AFM) ==  
 
== Atomic Force Microscopy (AFM) ==  
CNSI has a room devoted to AFM including 2 models Asylum and NanoScope. Contact Mark Cornish <cornish@engineering.ucsb.edu> to get tips and register. The cleanroom also has a NanoScope AFM.
+
CNSI has a room devoted to AFM including 2 models Asylum and NanoScope. Contact Mark Cornish <cornish@engineering.ucsb.edu> to get tips and register. The cleanroom also has a NanoScope AFM managed by Bill Mitchel <mitchell@ece.ucsb.edu>.
  
 
=== Asylum AFM ===
 
=== Asylum AFM ===

Revision as of 11:44, 18 November 2011

Materials Characterization

Atomic Force Microscopy (AFM)

CNSI has a room devoted to AFM including 2 models Asylum and NanoScope. Contact Mark Cornish <cornish@engineering.ucsb.edu> to get tips and register. The cleanroom also has a NanoScope AFM managed by Bill Mitchel <mitchell@ece.ucsb.edu>.

Asylum AFM

Asylum_AFM_MFC-3D_Procedure_v1_-_Basic_Tapping_Mode.docx

Asylum_AFM_MFC-3D_Procedure_v2_-_High_Resolution_Surface_Roughness_Scans_in_Attractive-Mode_Tapping.docx

NanoScope AFM

Bill will approve you to sign-up once someone he trusts trains you.

Analysis

Igor Pro demo: http://www.wavemetrics.com/support/demos.htm Asylum download requires a login, and to get one takes a little while. Is it possible to upload that to the wiki? Gwyddion and GTK+: http://gwyddion.net/download.php#stable-osx it recommends a specific GTK+, not sure why it matters though. If you have it from Pidgin or something I'm sure it'll work.

X-Ray Diffraction (XRD)

XRD qualification of wafer:

This is one scan in ~20minutes if you know the offcut and direction already.

  1. Note offcut amount and direction. Draw arrow relative to wafer flats. ([110] is the direction perpendicular to the major flat)
  2. ID the layer peak(s), if separated from the substrate peak, and give the strain(s) (or just peak separation)
  3. ID superlattice/QW fringes. Count them (e.g. -2 to +3) and note spacing in arcseconds
  4. Make note of any other strong fringe peaks or broad/mysterious layer peaks

NB: Offcut on GaAs may be up to 10degrees. (XRD person try a pole search to locate). InP offcut ~0.2degrees is standard and often not noticed during XRD.

Optical Characterization

LI curves

"Example:" This technique allows you to measure output power vs. injection current. The follwoing equipment is used:

  • Keithley (link to equipment)
  • Agilent powermeter (link)

The measurement can be controlled using this (link) software. A sample plot looks like this: (insert picture). More about this technique can be found in:

  1. Mr.X et al., IEEE Journ. of Lightwave Technol., vol. x, pp. xxx-xxx, Aug. 2005
  2. Our own uploaded description (in doc format maybe)

Electrical characterization

Analysis: http://gwyddion.net/download.php#stable-osx

Microwave measurements

Linearity measurements (OIP2, OIP3, SFDR,...)